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Application Of Vat Dyes

1.Procedure

1.1 Dip dyeing

Wetting with wat-->Dyeing-->Washing with cold water-->Oxidizing Washing with-->cold water-->Soaping-->Washing with hot water-->Washing with cold water-->Hydroextracting-->Drying.

1.2 Jip Dyeing

Wetting with water Dyeing Washing with cold water Oxidezing Soaping Washing with hot water Washing with cold water Drying.

1.3 Pad-Steam process

Pigment padding-->Drying-->Cooling-->Chemicals liquor padding-->Steaming -->Washing with cold water-->Oxidizing-->Washing-->Soaping-->Washing-->Drying

2.Pad-steaming recipes

Dyeing method Dyeing depth Sodium hydroxide(g/L) Sodium hydrosulphite 85%(g/L) Common salt or Sodium sulfate anhydrous(g/L) Steaming
Time(sec).
Steam temp.(oC)
Pad-
steam
Pale-Medimu 10-30 10-30 20-30 30-60 102-104
Medium-Deep 30-40 30-40 30-40

3.Stock Vatting recipes.

Method SV 1 SV II SV III
Liquor ratio 1:50 1:50 1:100
Sodium hydroxide 30%(ml/L) 60 30 60
Sodium hydrosulphite 85%(g/L) 15 10 15
Vatting temp.(oC) 60 50 60
Vatting time(min.) 10-15 10-15 10-15

4.Dyeing recipes

Dyeing conditon Amount dyestuff(weight on fiber)(%) Dyeing method
IN IW IK
0.1-1 1-3 3-6 0.1-1 1-3 3-6 0.1-1 1-3 3-6
Sodium hydroxide 30%(mL/L) 10-12 12-17 17-20 6-8 8-12 12-14 4-6 6-8 8-10
Sodium Hydrosulphite 85%(g/L) 4-5 5-7 7-8 3.5-4.5 4.5-6.5 6.5-7 4-5 5-7 7-8
Wetting agent 10%(mL/L) 5 5 5 5 5 5 5 5 5
Alcohol 95%(mL/L) 5 5 5 5 5 5 5 5 5
Sodium sulfate Anhydrous(g/L) - - - 5-10 10-15 15-25 5-10 10-15 15-25
Reduction temp.(oC) 60 50 50
Dyeing temp.(oC) 60 45-50 20-25

5.Oxidizing bath recipe

Method Sodium Perborate Hydrogen Peroxide 30% Potassium (Sodium bichromate)
Amount 3-4g/L 2-3mL/L 1-2g/L
Acetic acid Glacial - - 1-2mL/L
PH 10-11 9-10 -
Temp.(oC) 40-50 20-40 30-40
Time(min.) 10-20 10-20 10-20

6.Soaping bath recipe

Soap 3-5g/L
Sodium carbonate 2-3g/L
Temp. 98-100oC
Time 10-12min.
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